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master's thesis
Sinteza i spektroskopska karakterizacija simetričnih aminoskvareina
Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology, 2021. urn:nbn:hr:149:457863
Kamberovski, Nina
University of Zagreb
Faculty of Chemical Engineering and Technology

Institutional repository: Repository of Faculty of Chemical Engineering and Technology University of Zagreb

Cite this document

Kamberovski, N. (2021). Sinteza i spektroskopska karakterizacija simetričnih aminoskvareina (Master's thesis). Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:149:457863

Kamberovski, Nina. "Sinteza i spektroskopska karakterizacija simetričnih aminoskvareina." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2021. https://urn.nsk.hr/urn:nbn:hr:149:457863

Kamberovski, Nina. "Sinteza i spektroskopska karakterizacija simetričnih aminoskvareina." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2021. https://urn.nsk.hr/urn:nbn:hr:149:457863

Kamberovski, N. (2021). 'Sinteza i spektroskopska karakterizacija simetričnih aminoskvareina', Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, accessed 20 December 2024, https://urn.nsk.hr/urn:nbn:hr:149:457863

Kamberovski N. Sinteza i spektroskopska karakterizacija simetričnih aminoskvareina [Master's thesis]. Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology; 2021 [cited 2024 December 20] Available at: https://urn.nsk.hr/urn:nbn:hr:149:457863

N. Kamberovski, "Sinteza i spektroskopska karakterizacija simetričnih aminoskvareina", Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, 2021. Available at: https://urn.nsk.hr/urn:nbn:hr:149:457863

Metadata
TitleSinteza i spektroskopska karakterizacija simetričnih aminoskvareina
Title (english)Synthesis and spectroscopic characterization of symmetric aminosquaraines
AuthorNina Kamberovski
MentorDragana Vuk (mentor)
Committee memberDragana Vuk (predsjednik povjerenstva)
Committee memberVilko Mandić (član povjerenstva)
Committee memberIrena Škorić (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Chemical Engineering and Technology
Zagreb
Defense date and country2021-09-16, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract
Cilj ovog rada je pripremiti nove simetrične derivate skvareinske kiseline kroz nekoliko koraka. Prvi korak uključuje aminaciju početnog spoja 1-brom-3,5-dimetoksibenzena odgovarajućim aminom, pri čemu su dobiveni produkti 1 i 2. U drugom koraku se spojevi 1 i 2 podvrgavaju demetiliranju do alkoholnih derivata 3- 5. U posljednjem koraku dolazi do kondenzacije sa skvareinskom kiselinom te nastaju produkti 6- 8. U sklopu rada sintetiziran je i dialilni metoksi-derivat skvareinske kiseline 9, kako bi se dodatno ispitao utjecaj supstituenata na svojstva skvareina. Nadalje, svi produkti i međuprodukti u potpunosti su spektroskopski okarakterizirani.
Abstract (english)
The aim of this work is to prepare new symmetric derivatives of squaric acid through several steps. The first step involves amination of the starting compound 1-bromo-3,5-dimethoxybenzene with the appropriate amine to give products 1 and 2. In the second step, compounds 1 and 2 are demethylated to alcohol derivatives 3- 5. In the last step, condensation with squaric acid occurs and products 6-8 are formed. As part of the work, a diallyl methoxy derivative of squaric acid 9 was synthesized in order to further investigate the influence of substituents on the properties of squarein. Furthermore, all products and intermediates were fully spectroscopically characterized.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:149:457863
ProjectNumber: UIP-2019-04-2367
Title: Fenomeni na površini tijekom priprave naprednih nanokompozita infiltracijom i funkcionalizacijom poroznih materijala
Title: Surface limitations in preparing and infiltration of hard porous nanomaterial by soft or liquid precursors for performance enhancing
Acronym: SLIPPERYSLOPE
Leader: Vilko Mandić
Jurisdiction: Croatia
Funder: HRZZ
Funding stream: UIP
ProjectNumber: PZS-2019-02-1555
Title: Fotonaponska-geopolimerna fasada: uloga vode-kisika u naprednom sklapanju filmova kompozitnih materijala
Title: Photovoltaic-geopolymer facade: the water-oxygen role in the advanced assembly of layered composite materials
Acronym: PV-WALL
Leader: Vilko Mandić
Jurisdiction: Croatia
Funder: HRZZ
Funding stream: PZS
Study programmeTitle: Applied Chemistry - Graduate study; specializations in: Environmental chemistry and green technologies, Advanced materials and technologies, Applied organic chemistry
Course: Applied organic chemistry
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra primijenjene kemije (magistar/magistra primijenjene kemije)
Type of resourceText
File originBorn digital
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Created on2023-04-13 13:01:03