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undergraduate thesis
Priprava N,N-disupstituiranih derivata dimetoksianilina
Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology, 2020. urn:nbn:hr:149:245124
Marić, Marina Monika
University of Zagreb
Faculty of Chemical Engineering and Technology

Institutional repository: Repository of Faculty of Chemical Engineering and Technology University of Zagreb

Cite this document

Marić, M. M. (2020). Priprava N,N-disupstituiranih derivata dimetoksianilina (Undergraduate thesis). Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:149:245124

Marić, Marina Monika. "Priprava N,N-disupstituiranih derivata dimetoksianilina." Undergraduate thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2020. https://urn.nsk.hr/urn:nbn:hr:149:245124

Marić, Marina Monika. "Priprava N,N-disupstituiranih derivata dimetoksianilina." Undergraduate thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2020. https://urn.nsk.hr/urn:nbn:hr:149:245124

Marić, M. M. (2020). 'Priprava N,N-disupstituiranih derivata dimetoksianilina', Undergraduate thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, accessed 17 November 2024, https://urn.nsk.hr/urn:nbn:hr:149:245124

Marić MM. Priprava N,N-disupstituiranih derivata dimetoksianilina [Undergraduate thesis]. Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology; 2020 [cited 2024 November 17] Available at: https://urn.nsk.hr/urn:nbn:hr:149:245124

M. M. Marić, "Priprava N,N-disupstituiranih derivata dimetoksianilina", Undergraduate thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, 2020. Available at: https://urn.nsk.hr/urn:nbn:hr:149:245124

Metadata
TitlePriprava N,N-disupstituiranih derivata dimetoksianilina
Title (english)Preparation of the N,N-disubstituted derivatives of dimethoxyaniline
AuthorMarina Monika Marić
MentorDragana Vuk (mentor)
Committee memberDragana Vuk (predsjednik povjerenstva)
Committee memberIrena Škorić (član povjerenstva)
Committee memberVilko Mandić (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Chemical Engineering and Technology
Zagreb
Defense date and country2020-09-25, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract
U sklopu izrade ovog završnog rada proveden je niz pokušaja reakcije aminacije. Izučavane su reakcije sinteze potpomognute mikrovalovima, reakcije aminacije bez prisustva metalnih katalizatora, reakcije uz prisustvo n-BuLi, te reakcije alkiliranja. Kao najpogodnija metoda pokazala se reakcija uz n-BuLi pomoću koje su dobivena tri produkta u dobrom iskorištenju, N,N-diizobutil-3,5-dimetoksianilin (2), N,N-difenil-3,5-dimetoksianilin (3), te 1-(3,5-dimetoksifenil)piperidin (4). Osim spomenute metode, kao uspješna reakcija pokazala se i reakcija alkiliranja, odnosno metiliranja, čijom je primjenom dobiven N,N-dimetil-3,5-dimetoksianilin (6) u iskorištenju od 100%.
Abstract (english)
The aim of this work was to conduct a number of amination reaction attempts. A series of reactions have been studied, such as reactions using microwave irradiation, amination reactions without transition-metal catalyst, reactions using n-BuLi, and alkylation reactions. The most convenient method was the reaction using n-BuLi. The utilization of that method resulted in synthesis of three products in good yields, N,N-diisobutyl-3,5-dimethoxyaniline (2), N,N-diphenyl-3,5-dimethoxyaniline (3), te 1-(3,5-dimethoxyphenyl)piperidine (4). Besides the reaction with n-BuLi, methylation is another method that successfully produced a desired product, N,N-dimethyl-3,5-dimethoxyaniline (6) in 100% yield.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:149:245124
ProjectNumber: PZS-2019-02-1555
Title: Fotonaponska-geopolimerna fasada: uloga vode-kisika u naprednom sklapanju filmova kompozitnih materijala
Title: Photovoltaic-geopolymer facade: the water-oxygen role in the advanced assembly of layered composite materials
Acronym: PV-WALL
Leader: Vilko Mandić
Jurisdiction: Croatia
Funder: HRZZ
Funding stream: PZS
ProjectNumber: UIP-2019-04-2367
Title: Fenomeni na površini tijekom priprave naprednih nanokompozita infiltracijom i funkcionalizacijom poroznih materijala
Title: Surface limitations in preparing and infiltration of hard porous nanomaterial by soft or liquid precursors for performance enhancing
Acronym: SLIPPERYSLOPE
Leader: Vilko Mandić
Jurisdiction: Croatia
Funder: HRZZ
Funding stream: UIP
Study programmeTitle: Materials Science and Engineering - Undergraduate study
Study programme type: university
Study level: undergraduate
Academic / professional title: sveučilišni/a prvostupnik/ prvostupnica (baccalaureus/baccalaurea) inženjer/inženjerka kemijskog inženjerstva (sveučilišni/a prvostupnik/ prvostupnica (baccalaureus/baccalaurea) inženjer/inženjerka kemijskog inženjerstva)
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Created on2023-05-05 10:32:56