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undergraduate thesis
Sinteza Al2O3 sagorijevanjem uz asparagin kao gorivo
Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology, 2019. urn:nbn:hr:149:850710
Matančević, Ivona
University of Zagreb
Faculty of Chemical Engineering and Technology

Institutional repository: Repository of Faculty of Chemical Engineering and Technology University of Zagreb

Cite this document

Matančević, I. (2019). Sinteza Al2O3 sagorijevanjem uz asparagin kao gorivo (Undergraduate thesis). Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:149:850710

Matančević, Ivona. "Sinteza Al2O3 sagorijevanjem uz asparagin kao gorivo." Undergraduate thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2019. https://urn.nsk.hr/urn:nbn:hr:149:850710

Matančević, Ivona. "Sinteza Al2O3 sagorijevanjem uz asparagin kao gorivo." Undergraduate thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2019. https://urn.nsk.hr/urn:nbn:hr:149:850710

Matančević, I. (2019). 'Sinteza Al2O3 sagorijevanjem uz asparagin kao gorivo', Undergraduate thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, accessed 11 July 2024, https://urn.nsk.hr/urn:nbn:hr:149:850710

Matančević I. Sinteza Al2O3 sagorijevanjem uz asparagin kao gorivo [Undergraduate thesis]. Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology; 2019 [cited 2024 July 11] Available at: https://urn.nsk.hr/urn:nbn:hr:149:850710

I. Matančević, "Sinteza Al2O3 sagorijevanjem uz asparagin kao gorivo", Undergraduate thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, 2019. Available at: https://urn.nsk.hr/urn:nbn:hr:149:850710

Metadata
TitleSinteza Al2O3 sagorijevanjem uz asparagin kao gorivo
Title (english)Combustion synthesis of alumina using asparagine as a fuel
AuthorIvona Matančević
MentorStanislav Kurajica (mentor)
Committee memberStanislav Kurajica (predsjednik povjerenstva)
Committee memberVilko Mandić (član povjerenstva)
Committee memberGordana Matijašić (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Chemical Engineering and Technology
Zagreb
Defense date and country2019-09-19, Croatia
Scientific / art field,
discipline and subdiscipline		TECHNICAL SCIENCES
Basic Technical Sciences
Abstract
U ovom radu proučavani su procesi do kojih dolazi tijekom kristalizacije prašaka pripravljenih sintezom sagorijevanjem gdje su kao prekursori korišteni aluminijev nitrat nonahidrat kao oksidans i asparagin kao gorivo. Pripremljene su tri otopine s različitim omjerom goriva i oksidansa (suvišak goriva, stehiometrijski odnos i manjak goriva). Prašci pripravljeni sintezom sagorijevanjem analizirani su diferencijalnom toplinskom i termogravimetrijskom analizom (DTA/TGA), pretražnom elektronskom mikroskopijom (SEM), rendgenskom difrakcijom (XRD) i infracrvenom spektroskopijom s Fourierovom transformacijom (FTIR). Dobiveni rezultati pokazali su da vrijeme reakcije i temperatura sagorijevanja ovise o udjelu goriva. Uzorak s najvećim udjelom goriva imao je najvišu temperaturu sagorijevanja te je ta reakcija bila najprije gotova. Na kraju sinteze s gorivom u suvišku bilo je najmanje zaostale organske tvari. Kod uzorka s najmanje goriva zabilježeno je najkraće potrebno vrijeme na miješalici da bi došlo do početka sinteze te najveća količina zaostale organske tvari. Toplinskom obradom na 800°C uspješno je dobiven γ-Al2O3 kod sva tri uzorka.
Abstract (english)
In this work, the processes occurring in the course of powder crystallisation by combustion synthesis from precursor solutions containing aluminium nitrate nonahydrate as oxidant and asparagine as fuel were studied. Three solutions with different fuel-to-oxidizer ratio (fuel rich, stoichiometric and fuel lean) were prepared. Powders prepared by combustion synthesis were analysed by differential thermal and thermogravimetric analysis (DTA / TGA), scanning electron microscopy (SEM), X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR). Results have shown that reaction time and combustion temperature depend on the fuel content. The sample with the highest content of fuel had the shortest reaction time and highest combustion temperature. Also, it had the least residual organic matter after synthesis. The fuel deficient sample had the shortest mixing time needed for reaction and the most residual organic matter. γ-Al2O3 has been successfully obtained in all three samples with heat treatment at 800 °C.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:149:850710
Study programmeTitle: Applied Chemistry - Undergraduate study; specializations in: Environmental chemistry and green technologies, Advanced materials and technologies, Applied organic chemistry
Course: Advanced materials and technologies
Study programme type: university
Study level: undergraduate
Academic / professional title: sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) primijenjene kemije (sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) primijenjene kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
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Created on2023-05-26 08:01:40