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master's thesis
Kvantitativna energijski razlučujuća rendgenska spektrometrija
Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology, 2023. urn:nbn:hr:149:301580
Kliska, Ivana
University of Zagreb
Faculty of Chemical Engineering and Technology

Institutional repository: Repository of Faculty of Chemical Engineering and Technology University of Zagreb

Cite this document

Kliska, I. (2023). Kvantitativna energijski razlučujuća rendgenska spektrometrija (Master's thesis). Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:149:301580

Kliska, Ivana. "Kvantitativna energijski razlučujuća rendgenska spektrometrija." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2023. https://urn.nsk.hr/urn:nbn:hr:149:301580

Kliska, Ivana. "Kvantitativna energijski razlučujuća rendgenska spektrometrija." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2023. https://urn.nsk.hr/urn:nbn:hr:149:301580

Kliska, I. (2023). 'Kvantitativna energijski razlučujuća rendgenska spektrometrija', Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, accessed 26 November 2024, https://urn.nsk.hr/urn:nbn:hr:149:301580

Kliska I. Kvantitativna energijski razlučujuća rendgenska spektrometrija [Master's thesis]. Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology; 2023 [cited 2024 November 26] Available at: https://urn.nsk.hr/urn:nbn:hr:149:301580

I. Kliska, "Kvantitativna energijski razlučujuća rendgenska spektrometrija", Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, 2023. Available at: https://urn.nsk.hr/urn:nbn:hr:149:301580

Metadata
TitleKvantitativna energijski razlučujuća rendgenska spektrometrija
Title (english)Quantitative energy dispersive X-ray spectrometry
AuthorIvana Kliska
MentorJelena Macan (mentor)
Committee memberJelena Macan (predsjednik povjerenstva)
Committee memberJuraj Šipušić (član povjerenstva)
Committee memberAnamarija Rogina (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Chemical Engineering and Technology
Zagreb
Defense date and country2023-06-29, Croatia
Scientific / art field,
discipline and subdiscipline		TECHNICAL SCIENCES
Basic Technical Sciences
Abstract
Energijski razlučujuća rendgenska spektrometrija analitička je tehnika koja omogućuje identifikaciju kemijskih elemenata u uzorku pomoću pretražnog elektronskog mikroskopa. Ova tehnika detektira rendgenske zrake uzorka pobuđene snopom elektrona pretražnog elektronskog mikroskopa. Temelji se na spoznaji da je energija rendgenskih zraka povezana s atomskim brojem atoma, a njihov intenzitet s masenim udjelom atoma u uzorku. U ovom su radu uzorci poznatog i nepoznatog sastava karakterizirani pomoću pretražnog elektronskog mikroskopa te je na njima provedena energijski razlučujuća rendgenska spektrometrija. Dobiveni podaci prikazani su grafički, te su analizirani karakteristični maksimumi za pojedine elemente. Uspoređeni su rezultati računalne analize dobivene softverskom analizom podataka s grafičkom identifikacijom linija. Izračunati su množinski udjeli elemenata u spojevima uzoraka prema rezultatima računalne analize. Izvedena je korelacija između masenog sastava uzorka i odaziva dobivenog EDS analizom tako da su određeni Cliff-Lorimerovi faktori za pojedine elemente koji čine uzorke. Konačno, dan je zaključak o prednostima i nedostatcima te analitičke tehnike.
Abstract (english)
Energy dispersive X-ray spectrometry is an analytical technique that enables the identification of chemical elements in a sample using a scanning electron microscope. This technique detects X-rays from the sample during bombardment by an electron beam. Detected X-rays are related to the atomic number of atoms and their intensity to the mass fraction of atoms in the sample. In this work, samples of known and unknown composition were characterised using a scanning electron microscope and energy-dispersive X-ray spectrometry was performed on them. The obtained data are presented graphically, and the characteristic lines for individual elements are analyzed. The results of computer analysis obtained by software data analysis with graphic identification of peaks were compared. The mass fractions of the elements in the sample compounds were calculated according to the data obtained by the software analysis. The correlation between the mass composition of the sample and the response obtained by EDS analysis was performed, so that the Cliff-Lorimer factors were determined for the individual elements that make up the samples. Finally, a conclusion is given on the advantages and disadvantages of this analytical technique.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:149:301580
Study programmeTitle: Materials Science and Engineering - Graduate study
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra inženjer/inženjerka kemijskog inženjerstva (magistar/magistra inženjer/inženjerka kemijskog inženjerstva)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2023-07-26 10:46:20