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master's thesis
Primjena IC termografije pri očvršćivanju polimera u kalupima
Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology, 2017. urn:nbn:hr:149:684722
Pejnović, Martina
University of Zagreb
Faculty of Chemical Engineering and Technology

Institutional repository: Repository of Faculty of Chemical Engineering and Technology University of Zagreb

Cite this document

Pejnović, M. (2017). Primjena IC termografije pri očvršćivanju polimera u kalupima (Master's thesis). Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:149:684722

Pejnović, Martina. "Primjena IC termografije pri očvršćivanju polimera u kalupima." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2017. https://urn.nsk.hr/urn:nbn:hr:149:684722

Pejnović, Martina. "Primjena IC termografije pri očvršćivanju polimera u kalupima." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2017. https://urn.nsk.hr/urn:nbn:hr:149:684722

Pejnović, M. (2017). 'Primjena IC termografije pri očvršćivanju polimera u kalupima', Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, accessed 04 November 2024, https://urn.nsk.hr/urn:nbn:hr:149:684722

Pejnović M. Primjena IC termografije pri očvršćivanju polimera u kalupima [Master's thesis]. Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology; 2017 [cited 2024 November 04] Available at: https://urn.nsk.hr/urn:nbn:hr:149:684722

M. Pejnović, "Primjena IC termografije pri očvršćivanju polimera u kalupima", Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, 2017. Available at: https://urn.nsk.hr/urn:nbn:hr:149:684722

Metadata
TitlePrimjena IC termografije pri očvršćivanju polimera u kalupima
Title (english)Application of IC thermography during polymer curing in molds
AuthorMartina Pejnović
MentorVanja Kosar (mentor)
Committee memberVanja Kosar (predsjednik povjerenstva)
Committee memberNenad Bolf (član povjerenstva)
Committee memberZoran Mandić (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Chemical Engineering and Technology
Zagreb
Defense date and country2017-09-29, Croatia
Scientific / art field,
discipline and subdiscipline		TECHNICAL SCIENCES
Chemical Engineering
Reaction Engineering
Abstract
U ovom radu provedena je analiza procesa očvršćivanja poliesterske smole u valjkastom kalupu grijanim zrakom i mineralnim uljem. Praćen je prijenos topline u uzorku smole eksperimentalno te pomoću matematičkog modela. Eksperimentalno se pratila promjena temperature u centru kalupa s vremenom reakcije te se uzorak podvrgnuo mjerenjima u diferencijalnom pretražnom kalorimetru pri dinamičkim i izotermnim uvjetima. Rezultati pretražne kalorimetrije daju nam ukupnu toplinu reakcije te bolji uvid u kinetiku reakcije. Matematički model procesa sastoj se od bilance topline, bilance tvari te kinetičkog modela koji povezuje bilancu topline i bilancu tvari. Navedeni skup diferencijalnih jednadžbi rješava se matematički i uspoređuje s rezultatima dobivenim eksperimentom. Pokazalo se da predloženi matematički model dobro opisuje eksperimentalno izmjerene temperature u centru klupa. Prijenos topline praćen je i infracrvenom termografijom pri čemu je snimana promjena temperature s napredovanjem reakcije i temperaturni gradijent po radijalnom presjekom kalupa. Sve navedene metode daju nam potpuniju sliku procesa očvršćivanja poliesterskih smola što je iznimno korisno prilikom modeliranja procesa izrade proizvoda od poliesterskih smola.
Abstract (english)
The cure of unsaturated polyester was studied by using cylindrical mould heated with hot air and mineral oil. Analysis consist an experimental measurement and mathematical model. Temperature changes in centre of the mould vs. reaction time were experimentally followed and differential scanning calorimeter measurements in dynamic and isothermal conditions were taken. DSC measurements gave us total reaction heat as well as better insight in the reaction kinetics. Mathematical model is consisted of heat and mass balance as well as the kinetic model witch bonds both balance. The named differential equations were solved mathematically and compared with the experimental results. It has been shown that given mathematical model shows good agreement with experimental result. The heat transfer was monitored with IC thermograph where the temperature changes on the surface of the mould and on the radial cut. All mentioned methods give more complete image of the curing process and they are very helpful for modelling of resin production process.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:149:684722
Study programmeTitle: Applied Chemistry - Graduate study; specializations in: Environmental chemistry and green technologies, Advanced materials and technologies, Applied organic chemistry
Course: Advanced materials and technologies
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra primijenjene kemije (magistar/magistra primijenjene kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2020-04-30 12:27:57