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master's thesis
Priprema na zraku stabilnih bakrovih nanočestica za ispis tintnim pisačem
Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology, 2019. urn:nbn:hr:149:534114
Dragoš, Matea
University of Zagreb
Faculty of Chemical Engineering and Technology

Institutional repository: Repository of Faculty of Chemical Engineering and Technology University of Zagreb

Cite this document

Dragoš, M. (2019). Priprema na zraku stabilnih bakrovih nanočestica za ispis tintnim pisačem (Master's thesis). Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:149:534114

Dragoš, Matea. "Priprema na zraku stabilnih bakrovih nanočestica za ispis tintnim pisačem." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2019. https://urn.nsk.hr/urn:nbn:hr:149:534114

Dragoš, Matea. "Priprema na zraku stabilnih bakrovih nanočestica za ispis tintnim pisačem." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2019. https://urn.nsk.hr/urn:nbn:hr:149:534114

Dragoš, M. (2019). 'Priprema na zraku stabilnih bakrovih nanočestica za ispis tintnim pisačem', Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, accessed 01 June 2024, https://urn.nsk.hr/urn:nbn:hr:149:534114

Dragoš M. Priprema na zraku stabilnih bakrovih nanočestica za ispis tintnim pisačem [Master's thesis]. Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology; 2019 [cited 2024 June 01] Available at: https://urn.nsk.hr/urn:nbn:hr:149:534114

M. Dragoš, "Priprema na zraku stabilnih bakrovih nanočestica za ispis tintnim pisačem", Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, 2019. Available at: https://urn.nsk.hr/urn:nbn:hr:149:534114

Metadata
TitlePriprema na zraku stabilnih bakrovih nanočestica za ispis tintnim pisačem
Title (english)Formation of air-stable copper nanoparticles for inkjet printing
AuthorMatea Dragoš
MentorStjepan Milardović (mentor)
Committee memberStjepan Milardović (predsjednik povjerenstva)
Committee memberPetar Kassal (član povjerenstva)
Committee memberZoran Mandić (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Chemical Engineering and Technology
Zagreb
Defense date and country2019-09-26, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract
Glavni cilj nanotehnologije je formiranje uzoraka materijala s potpuno novim i drugačijim svojstvima u odnosu na uzorke u makro obliku. Istraživanja u području sinteze nanočestica metala vrlo su zanimljiva sa znanstvenog i industrijskog aspekta. Predmet istraživanja ovog diplomskog rada je priprema nanočestica bakra stabilnih na zraku i pogodnih za ispis uporabom tintnog pisača. Nanočestice bakra sintetizirane su metodom kemijske redukcije iz vodene otopine, uporabom različitih prekursora i redukcijskih sredstava. Prekursori koji su korišteni su soli Cu(Ac)2, Cu(NO3)2 i Cu(SO4)2, te dva redukcijska sredstva N2H4 i NaBH4. Površina nanočestica bakra zaštićena je slojem elementarnog srebra kako bi se spriječila oksidacija bakra u procesu sinteriranja. Uvjeti sinteze sistematski su mijenjani kako bi se provjerio njihov utjecaj na veličinu nastalih nanočestica i na kinetiku kemijske reakcije. Nastale nanočestice karakterizirane su primjenom UV-Vis spektrofotometrije i cikličke voltametrije.
Abstract (english)
The main objective of nanotechnology is the formation of materials with different, novel properties compared to their macro-sized counterparts. During the last decade, synthetic methods for the preparation of metallic nanoparticles represent one of the most investigated research field. The main subject of research in this thesis is preparation of air-stable copper nanoparticles suitable for inkjet printing technology. Copper nanoparticles have been synthesized by the chemical reduction method from aqueous solutions, using different precursors and reducing agents. Different copper(II) saltes were used as a precursor specimens: acetate, nitrate and sulfate. Besides precursor molecule, two fast-kinetic inorganic compounds, N2H4 and NaBH4, were examined as the reducing agents. The surface of the copper nanoparticles was covered with metalic silver layer in order to protect grains from further oxidation during sintering process. Synthesis conditions are systematically modified to check their effects on the size of the formed nanoparticles and on the kinetics of chemical reactions. The resulting nanoparticles were characterized by UV-Vis spectrophotometry and cyclic voltammetry.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:149:534114
Study programmeTitle: Applied Chemistry - Graduate study; specializations in: Environmental chemistry and green technologies, Advanced materials and technologies, Applied organic chemistry
Course: Advanced materials and technologies
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra primijenjene kemije (magistar/magistra primijenjene kemije)
Type of resourceText
File originBorn digital
Access conditionsClosed access
Terms of useLicence In copyright icon
Created on2022-02-17 09:35:29