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master's thesis
Sinteza zeolita u prisutnosti algi Chlorella vulgaris i Dunaliella tertiolecta
Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology, 2019. urn:nbn:hr:149:353967
Fiolić, Tamara
University of Zagreb
Faculty of Chemical Engineering and Technology

Institutional repository: Repository of Faculty of Chemical Engineering and Technology University of Zagreb

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Fiolić, T. (2019). Sinteza zeolita u prisutnosti algi Chlorella vulgaris i Dunaliella tertiolecta (Master's thesis). Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:149:353967

Fiolić, Tamara. "Sinteza zeolita u prisutnosti algi Chlorella vulgaris i Dunaliella tertiolecta." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2019. https://urn.nsk.hr/urn:nbn:hr:149:353967

Fiolić, Tamara. "Sinteza zeolita u prisutnosti algi Chlorella vulgaris i Dunaliella tertiolecta." Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, 2019. https://urn.nsk.hr/urn:nbn:hr:149:353967

Fiolić, T. (2019). 'Sinteza zeolita u prisutnosti algi Chlorella vulgaris i Dunaliella tertiolecta', Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, accessed 26 December 2024, https://urn.nsk.hr/urn:nbn:hr:149:353967

Fiolić T. Sinteza zeolita u prisutnosti algi Chlorella vulgaris i Dunaliella tertiolecta [Master's thesis]. Zagreb: University of Zagreb, Faculty of Chemical Engineering and Technology; 2019 [cited 2024 December 26] Available at: https://urn.nsk.hr/urn:nbn:hr:149:353967

T. Fiolić, "Sinteza zeolita u prisutnosti algi Chlorella vulgaris i Dunaliella tertiolecta", Master's thesis, University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, 2019. Available at: https://urn.nsk.hr/urn:nbn:hr:149:353967

Metadata
TitleSinteza zeolita u prisutnosti algi Chlorella vulgaris i Dunaliella tertiolecta
Title (english)Zeolite synthesis in the presence of algae Chlorella vulgaris and Dunaliella tertiolecta
AuthorTamara Fiolić
MentorJuraj Šipušić (mentor)
Committee memberJuraj Šipušić (predsjednik povjerenstva)
Committee memberHelena Otmačić Ćurković (član povjerenstva)
Committee memberDajana Kučić Grgić (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Chemical Engineering and Technology
Zagreb
Defense date and country2019-09-16, Croatia
Scientific / art field,
discipline and subdiscipline		TECHNICAL SCIENCES
Chemical Engineering
Abstract
Zeoliti su kristalni hidratizirani alumosilikati alkalijskih i zemnoalkalijskih metala opće formule M2/nO × Al2O3 × x SiO2 × y H2O. Industrijski su vrlo važni materijali koji se koriste kao ionski izmjenjivači, molekularna sita, katalizatori, deterdženti, itd. U ovom radu sintetiziran je zeolit Silikalit-1(strukturni tip MFI) pri temperaturama 100 °C i 150 °C te pri različitim vremenima sinteze. Sinteza je provedena u prisutnosti prirodnih sirovina, algi Chlorella vulgaris i Dunaliella tertiolecta. Pripremljenim uzorcima zeolita određena je veličina čestica te ovisnost volumnog udjela o veličini čestica (Masterseizer). Kemijski sastav elemenata prisutnih u uzorcima zeolita određen je pomoću EDX analize dok su funkcionalne skupine karakteristične za zeolite identificirane infracrvenom spektroskopijom. Pomoću optičkog i pretražnog elektronskog mikroskopa snimljene su fotografije odnosno mikrografije uzoraka. Iz rezultata je vidljivo da su čestice zeolita različitih veličina i oblika. Najzastupljeniji elementi prisutni u uzorcima zeolita su silicij i kisik, dok su manje zastupljeni elementi Ca, Mg, F, Na i P. Vrpce snimljene FTIR spektrometrijom odgovaraju vezama Si-O, Si-O-Si i Si-O-Al.
Abstract (english)
Zeolites are crystalline hydrated alumosilicates of alkali and alkaline earth metals of the general formula M2/nO × Al2O3 × x SiO2 × y H2O. They are very important industrial materials that are used as ion exchangers, molecular sieves, catalysts, detergents, etc. In this paper Zeolite Silicalite-1 (structural tip of MFI) was synthesized at temperatures of 100 °C and 150 °C at different times of the synthesis. The synthesis was carried out in the presence of natural raw materials, algae Chlorella vulgaris and Dunaliella tertiolecta. The prepared zeolite samples were characterized by the particle size and the dependence of the volume fraction of the particle size (Masterseizer). The chemical compositions of the elements present in the zeolite samples is determined by EDX analysis, while the functional groups characteristic to the zeolite are identified by infrared spectroscopy. Photographs and micrographs of the samples were taken using an optical and scanning electron microscope. The results show that zeolite particles are of different sizes and shapes. The most abundant elements present in the zeolite samples are silicon and oxygen, while the less represented elements are Ca, Mg, F, Na, and P. The bands recorded by FTIR spectrometry correspond to the Si-O, Si-O-Si, and Si-O-Al bonds.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:149:353967
Study programmeTitle: Materials Science and Engineering - Graduate study
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra inženjer/inženjerka kemijskog inženjerstva (magistar/magistra inženjer/inženjerka kemijskog inženjerstva)
Type of resourceText
File originBorn digital
Access conditionsOpen access
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Created on2022-02-17 11:59:27