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master's thesis
Utjecaj aniona na molekulsku i kristalnu građu srebrovih kompleksa s makrocikličkim Schiffovim bazama
Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2022. urn:nbn:hr:182:345286
Šebalj, Lorena
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry

Institutional repository: Repository of the Department of Chemistry, Osijek

Cite this document

Šebalj, L. (2022). Utjecaj aniona na molekulsku i kristalnu građu srebrovih kompleksa s makrocikličkim Schiffovim bazama (Master's thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:345286

Šebalj, Lorena. "Utjecaj aniona na molekulsku i kristalnu građu srebrovih kompleksa s makrocikličkim Schiffovim bazama." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2022. https://urn.nsk.hr/urn:nbn:hr:182:345286

Šebalj, Lorena. "Utjecaj aniona na molekulsku i kristalnu građu srebrovih kompleksa s makrocikličkim Schiffovim bazama." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2022. https://urn.nsk.hr/urn:nbn:hr:182:345286

Šebalj, L. (2022). 'Utjecaj aniona na molekulsku i kristalnu građu srebrovih kompleksa s makrocikličkim Schiffovim bazama', Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 27 November 2024, https://urn.nsk.hr/urn:nbn:hr:182:345286

Šebalj L. Utjecaj aniona na molekulsku i kristalnu građu srebrovih kompleksa s makrocikličkim Schiffovim bazama [Master's thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2022 [cited 2024 November 27] Available at: https://urn.nsk.hr/urn:nbn:hr:182:345286

L. Šebalj, "Utjecaj aniona na molekulsku i kristalnu građu srebrovih kompleksa s makrocikličkim Schiffovim bazama", Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2022. Available at: https://urn.nsk.hr/urn:nbn:hr:182:345286

Metadata
TitleUtjecaj aniona na molekulsku i kristalnu građu srebrovih kompleksa s makrocikličkim Schiffovim bazama
Title (english)Influence of anions on the molecular and crystal structure of silver complexes with macrocyclic Schiff bases
AuthorLorena Šebalj
MentorTomislav Balić (mentor)
Committee memberOlivera Galović (predsjednik povjerenstva)
Committee memberTomislav Balić (član povjerenstva)
Committee memberAleksandar Sečenji (član povjerenstva)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry)
Osijek
Defense date and country2022-07-11, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Inorganic Chemistry
Abstract
Predmet istraživanja ovog diplomskog rada je utjecaj aniona na molekulsku i kristalnu građu srebrovih kompleksa sa makrocikličkim Schiffovim bazama. Pripremljena je makrociklička Schiffova baza koja je služila kao ligand, a kao metalne soli prijelaznih elemenata koristili su se srebrov perklorat (AgClO4), srebrov heksafluorofosfat (AgPF6). srebrov heksafluoroantimonat (AgSbF6) i srebrov tetrafluoroborat (AgBF4). Priprava srebrovih kompleksa izvedena je uz odgovarajući ligand i metalni kation u U-cijevi uz diklormetan i metanol kao otapalo. Od izvedenih sinteza uspješno su izolirane i identificirane 4 nove kristalne strukture. Dobiveni spojevi su karakterizirani IR spektroskopijom (FT-IR), a molekulske i kristalne strukture određene su rendgenskom difrakcijom.
Abstract (english)
The subject of this thesis is the influence of anions on the molecular and crystal structure of silver complexes with macrocyclic Schiff bases. A prepared macrocyclic Schiff base served as a ligand, and silver perchlorate (AgClO4), silver hexafluorophosphate (AgPF6), silver hexafluoroantimonate (AgSbF6) and silver tetrafluoroborate (AgBF4) were used as metal salts. Preparation of silver complexes was performed with the appropriate ligand and metal salt in a U-shaped tube with dichloromethane and methanol as solvent. From the performed syntheses, 4 new crystal structures were successfully isolated and identified. The obtained compounds were characterized by IR spectroscopy (FT-IR), and molecular and crystal structures were determined by X-ray diffraction.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:345286
Study programmeTitle: Graduate University Study of Chemistry; research program; specializations in: Research program
Course: Research program
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra kemije (magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2022-08-08 07:59:54