prikaz prve stranice dokumenta Active modulation in neat carbon dioxide packed column comprehensive two-dimensional supercritical fluid chromatography
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Scientific paper - Original scientific paper
Active modulation in neat carbon dioxide packed column comprehensive two-dimensional supercritical fluid chromatography
Journal of Chromatography A, 1536 (2018); 176-184. https://doi.org/10.1016/j.chroma.2017.08.063
Petković, Orjen; Guibal, Pierre; Sassiat, Patrick; Vial, Jérôme; Thiébaut, Didier

Institutional repository: Repository of the University of Rijeka, Faculty of Medicine

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Petković, O., Guibal, P., Sassiat, P., Vial, J. & Thiébaut, D. (2018). Active modulation in neat carbon dioxide packed column comprehensive two-dimensional supercritical fluid chromatography. Journal of Chromatography A, 1536., 176-184. doi: 10.1016/j.chroma.2017.08.063

Petković, Orjen, et al. "Active modulation in neat carbon dioxide packed column comprehensive two-dimensional supercritical fluid chromatography." Journal of Chromatography A, vol. 1536, 2018, pp. 176-184. https://doi.org/10.1016/j.chroma.2017.08.063

Petković, Orjen, Pierre Guibal, Patrick Sassiat, Jérôme Vial and Didier Thiébaut. "Active modulation in neat carbon dioxide packed column comprehensive two-dimensional supercritical fluid chromatography." Journal of Chromatography A 1536 (2018): 176-184. https://doi.org/10.1016/j.chroma.2017.08.063

Petković, O., et al. (2018) 'Active modulation in neat carbon dioxide packed column comprehensive two-dimensional supercritical fluid chromatography', Journal of Chromatography A, 1536, pp. 176-184. doi: 10.1016/j.chroma.2017.08.063

Petković O, Guibal P, Sassiat P, Vial J, Thiébaut D. Active modulation in neat carbon dioxide packed column comprehensive two-dimensional supercritical fluid chromatography. Journal of Chromatography A [Internet]. 2018 February [cited 2024 November 26];1536:176-184. doi: 10.1016/j.chroma.2017.08.063

O. Petković, P. Guibal, P. Sassiat, J. Vial and D. Thiébaut, "Active modulation in neat carbon dioxide packed column comprehensive two-dimensional supercritical fluid chromatography", Journal of Chromatography A, vol. 1536, pp. 176-184, February 2018. [Online]. Available at: https://urn.nsk.hr/urn:nbn:hr:184:832400. [Accessed: 26 November 2024]

Metadata
Title (english)Active modulation in neat carbon dioxide packed column comprehensive two-dimensional supercritical fluid chromatography
AuthorOrjen Petković
AuthorPierre Guibal
AuthorPatrick Sassiat
AuthorJérôme Vial
AuthorDidier Thiébaut
Author's institutionUniversity of Rijeka
Faculty of Medicine
(Department of Chemistry and Biochemistry)
Scientific / art field,
discipline and subdiscipline		BIOMEDICINE AND HEALTHCARE
Basic Medical Sciences
Medical Biochemistry
Abstract (english)
After demonstrating in a first paper the feasibility of SFCxSFC without decompression of the mobile phase, a modified interface has been developed in order to perform active modulation between the two SFC dimensions. In this paper, it is shown that the new interface enabled independent control of modulation parameters in SFCxSFC and performed a band compression effect of solutes between the two SFC dimensions. The effectiveness of this new modulation process was studied using a Design of Experiments. The SFCxSFC prototype was applied to the analysis of a real oil sample to demonstrate the benefits of the active modulator; in comparison to our previous results obtained without active modulation, better separation was obtained with the new interface owing to the peak compression occurring in the modulator.
Keywords (english)
Languageenglish
Publication typeScientific paper - Original scientific paper
Publication statusPublished
Peer reviewPeer review - international
Publication versionAccepted version
Journal titleJournal of Chromatography A
Numberingvol. 1536, pp. 176-184
p-ISSN0021-9673
DOIhttps://doi.org/10.1016/j.chroma.2017.08.063
URN:NBNurn:nbn:hr:184:832400
Publication2018-02
Document URLhttps://linkinghub.elsevier.com/retrieve/pii/S0021967317312414
Type of resourceText
Access conditionsOpen access
Terms of useLicence Attribution-NonCommercial-NoDerivatives 4.0 International (CC BY-NC-ND 4.0) icon
Created on2022-02-04 07:59:20