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master's thesis
Istraživanje mehanokemijske sinteze kokristala in situ Ramanovom spektroskopijom
Zagreb: University of Zagreb, Faculty of Science, 2016. urn:nbn:hr:217:200111
Lukin, Stipe
University of Zagreb
Faculty of Science
Department of Chemistry

Institutional repository: Repository of the Faculty of Science

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Lukin, S. (2016). Istraživanje mehanokemijske sinteze kokristala in situ Ramanovom spektroskopijom (Master's thesis). Zagreb: University of Zagreb, Faculty of Science. Retrieved from https://urn.nsk.hr/urn:nbn:hr:217:200111

Lukin, Stipe. "Istraživanje mehanokemijske sinteze kokristala in situ Ramanovom spektroskopijom." Master's thesis, University of Zagreb, Faculty of Science, 2016. https://urn.nsk.hr/urn:nbn:hr:217:200111

Lukin, Stipe. "Istraživanje mehanokemijske sinteze kokristala in situ Ramanovom spektroskopijom." Master's thesis, University of Zagreb, Faculty of Science, 2016. https://urn.nsk.hr/urn:nbn:hr:217:200111

Lukin, S. (2016). 'Istraživanje mehanokemijske sinteze kokristala in situ Ramanovom spektroskopijom', Master's thesis, University of Zagreb, Faculty of Science, accessed 22 November 2024, https://urn.nsk.hr/urn:nbn:hr:217:200111

Lukin S. Istraživanje mehanokemijske sinteze kokristala in situ Ramanovom spektroskopijom [Master's thesis]. Zagreb: University of Zagreb, Faculty of Science; 2016 [cited 2024 November 22] Available at: https://urn.nsk.hr/urn:nbn:hr:217:200111

S. Lukin, "Istraživanje mehanokemijske sinteze kokristala in situ Ramanovom spektroskopijom", Master's thesis, University of Zagreb, Faculty of Science, Zagreb, 2016. Available at: https://urn.nsk.hr/urn:nbn:hr:217:200111

Metadata
TitleIstraživanje mehanokemijske sinteze kokristala in situ Ramanovom spektroskopijom
Title (english)Mechanochemical cocrystal formation studied by in situ Raman spectroscopy.
AuthorStipe Lukin
MentorIvan Halasz (mentor)
Committee memberJosip Požar (predsjednik povjerenstva)
Committee memberIvica Đilović (član povjerenstva)
Committee memberBranimir Bertoša (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Science
(Department of Chemistry)
Zagreb
Defense date and country2016-07-08, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract
U ovom radu mehanokemijskom sintezom u suhim uvjetima i tekućinom potpomognutim mljevenjem dobiveni su kokristali nikotinamida s benzojevom, antranilnom ili salicilnom kiselinom. Kokristali s antranilnom i benzojevom kiselinom dosad nisu bili poznati u literaturi i okarakterizirani su uz pomoć difrakcije rendgenskih zraka na praškastim uzorcima i uz pomoć Ramanove spektroskopije. Kristalne strukture dosad nepoznatih kokristala određene su iz difrakcijskih podataka. In situ Ramanovom spektroskopijom praćene su sve reakcije, a istraţio se i utjecaj dodatka male količine primarnih alkohola na brzinu i tijek reakcije.
Abstract (english)
In this thesis neat grinding and liquid-assisted grinding procedures for mechanochemical synthesis of cocrystals of nicotinamide with benzoic, anthranillic or salicylic acid were investigated. Obtained cocrystals of nicotinamide with benzoic or anthranillic acid were not previously known in the literature and were charachterized using powder X-ray diffraction and Raman spectroscopy. Crystal structures were solved using powder X-ray diffraction data. In situ Raman spectroscopy was used to gain insights into the course of the reaction including the influence of small quantities of added alcohols.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:217:200111
Study programmeTitle: Graduate Studies in Chemistry; specializations in: Research (scientific-professional) programme
Course: Research (scientific-professional) programme
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra kemije (magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
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Created on2017-01-26 13:26:30