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master's thesis
Sinteza i struktura kokristala o-hidroksi imina povezanih halogenskom vezom
Zagreb: University of Zagreb, Faculty of Science, 2016. urn:nbn:hr:217:846825
Nogalo, Ivana
University of Zagreb
Faculty of Science
Department of Chemistry

Institutional repository: Repository of the Faculty of Science

Cite this document

Nogalo, I. (2016). Sinteza i struktura kokristala o-hidroksi imina povezanih halogenskom vezom (Master's thesis). Zagreb: University of Zagreb, Faculty of Science. Retrieved from https://urn.nsk.hr/urn:nbn:hr:217:846825

Nogalo, Ivana. "Sinteza i struktura kokristala o-hidroksi imina povezanih halogenskom vezom." Master's thesis, University of Zagreb, Faculty of Science, 2016. https://urn.nsk.hr/urn:nbn:hr:217:846825

Nogalo, Ivana. "Sinteza i struktura kokristala o-hidroksi imina povezanih halogenskom vezom." Master's thesis, University of Zagreb, Faculty of Science, 2016. https://urn.nsk.hr/urn:nbn:hr:217:846825

Nogalo, I. (2016). 'Sinteza i struktura kokristala o-hidroksi imina povezanih halogenskom vezom', Master's thesis, University of Zagreb, Faculty of Science, accessed 25 November 2024, https://urn.nsk.hr/urn:nbn:hr:217:846825

Nogalo I. Sinteza i struktura kokristala o-hidroksi imina povezanih halogenskom vezom [Master's thesis]. Zagreb: University of Zagreb, Faculty of Science; 2016 [cited 2024 November 25] Available at: https://urn.nsk.hr/urn:nbn:hr:217:846825

I. Nogalo, "Sinteza i struktura kokristala o-hidroksi imina povezanih halogenskom vezom", Master's thesis, University of Zagreb, Faculty of Science, Zagreb, 2016. Available at: https://urn.nsk.hr/urn:nbn:hr:217:846825

Metadata
TitleSinteza i struktura kokristala o-hidroksi imina povezanih halogenskom vezom
Title (english)Synthesis and structure of halogen bonded cocrystals of an o-hydroxy imine
AuthorIvana Nogalo
MentorDominik Cinčić (mentor)
Committee memberDominik Cinčić (predsjednik povjerenstva)
Committee memberSanda Rončević (član povjerenstva)
Committee memberJosip Požar (član povjerenstva)
Committee memberVladimir Stilinović (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Science
(Department of Chemistry)
Zagreb
Defense date and country2016-09-16, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Inorganic Chemistry
Abstract
U sklopu ovog diplomskog rada pripravljen je imin kondezacijom o-vanilina i 4-aminobenzonitrila. Mehanokemijskom sintezom, sintezom iz otopine i metodom ubrzanog starenja izučavana je mogućnost nastajanja kokristala molekule imina s odabranim donorima halogenske veze: 1,2- i 1,4-dijodtetrafluorbenzenom. Pripravljeni kokristali izučavani su metodom difrakcije rentgenskih zraka na praškastom uzorku, termogravimetrijom i razlikovno-pretražnom kalorimetrijom. Za oba pripravljena kokristala metodom difrakcije rentgenskog zračenja na jediničnom kristalu iznađena je molekulska i kristalna struktura, te je ista dovedena u vezu s njihovim termičkim svojstvima.
Abstract (english)
Within this master thesis an imine was prepared through condensation of o-vanillin and 4-aminobenzonitrile. The possibility of cocrystallization of the selected imine and two halogen bond donors (1,2- and 1,4-diiodotetrafluorobenzene) was investigated by means of mechanochemical synthesis, solution based synthesis and accelerated ageing. The cocrystals were described by powder X-ray diffraction, thermogravimetry and differential scanning calorimetry. The crystal and molecular structures of two prepared compounds were explored by single crystal X-ray diffraction, and correlated with thermal properties.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:217:846825
Study programmeTitle: Graduate university studies in chemistry; specializations in: Research programme
Course: Research programme
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra kemije (magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2017-01-27 10:39:52