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master's thesis
Sinteza i karakterizacija aromatskih azodioksidnih i azo polimera
Zagreb: University of Zagreb, Faculty of Science, 2019. urn:nbn:hr:217:736976
Ruklin, Paula
University of Zagreb
Faculty of Science
Department of Chemistry

Institutional repository: Repository of the Faculty of Science

Cite this document

Ruklin, P. (2019). Sinteza i karakterizacija aromatskih azodioksidnih i azo polimera (Master's thesis). Zagreb: University of Zagreb, Faculty of Science. Retrieved from https://urn.nsk.hr/urn:nbn:hr:217:736976

Ruklin, Paula. "Sinteza i karakterizacija aromatskih azodioksidnih i azo polimera." Master's thesis, University of Zagreb, Faculty of Science, 2019. https://urn.nsk.hr/urn:nbn:hr:217:736976

Ruklin, Paula. "Sinteza i karakterizacija aromatskih azodioksidnih i azo polimera." Master's thesis, University of Zagreb, Faculty of Science, 2019. https://urn.nsk.hr/urn:nbn:hr:217:736976

Ruklin, P. (2019). 'Sinteza i karakterizacija aromatskih azodioksidnih i azo polimera', Master's thesis, University of Zagreb, Faculty of Science, accessed 30 December 2024, https://urn.nsk.hr/urn:nbn:hr:217:736976

Ruklin P. Sinteza i karakterizacija aromatskih azodioksidnih i azo polimera [Master's thesis]. Zagreb: University of Zagreb, Faculty of Science; 2019 [cited 2024 December 30] Available at: https://urn.nsk.hr/urn:nbn:hr:217:736976

P. Ruklin, "Sinteza i karakterizacija aromatskih azodioksidnih i azo polimera", Master's thesis, University of Zagreb, Faculty of Science, Zagreb, 2019. Available at: https://urn.nsk.hr/urn:nbn:hr:217:736976

Metadata
TitleSinteza i karakterizacija aromatskih azodioksidnih i azo polimera
Title (english)Synthesis and characterization of aromatic azodioxy and azo polymers
AuthorPaula Ruklin
MentorIvana Biljan (mentor)
Committee memberIvana Biljan (predsjednik povjerenstva)
Committee memberSnežana Miljanić (član povjerenstva)
Committee memberBiserka Prugovečki (član povjerenstva)
Committee memberVesna Petrović Peroković (član povjerenstva)
GranterUniversity of Zagreb
Faculty of Science
(Department of Chemistry)
Zagreb
Defense date and country2019-12-06, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract
U sklopu ovog diplomskog rada, provedena je sinteza i karakterizacija novog aromatskog tetranitrozo/azodioksidnog spoja i novih aromatskih azo kovalentnih organskih polimera. Aromatski tetranitrozo spoj sintetiziran je oksidacijom odgovarajućeg aromatskog tetraamino spoja i okarakteriziran spektroskopijom NMR u otopini. Aromatski azo polimeri priređeni su reakcijom kondenzacije aromatskih tetranitro i tetraamino spojeva odnosno tetranitro i odabranih diamino spojeva u bazičnim uvjetima. Strukturne karakteristike i termička svojstva aromatskih azo polimera proučena su tehnikama IR spektroskopije, difrakcijom rendgenskog zračenja na polikristalnom uzorku i termogravimetrijskom analizom. Usporedba IR spektara te difraktograma polikristalnih uzoraka polaznih spojeva i dobivenih produkata ukazuje na nastanak amorfnih aromatskih azo polimera.
Abstract (english)
Within this diploma thesis, the synthesis and characterization of novel aromatic tetranitroso/azodioxide compound and azo covalent organic polymers was performed. The aromatic tetranitroso compound was synthesized by oxidation of the corresponding aromatic tetraamino compound and characterized by NMR spectroscopy in solution. Aromatic azo polymers were prepared by condensation reaction of aromatic tetranitro and tetraamino compounds, and tetranitro and selected diamino compounds under basic conditions. The structural characteristics and thermal properties of aromatic azo polymers were studied by IR spectroscopy, X-ray powder diffraction and thermogravimetric analysis. Comparison of IR spectra and X-ray powder diffractograms of starting compounds and obtained products indicated formation of amorphous aromatic azo polymers.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:217:736976
Study programmeTitle: Graduate university studies in chemistry; specializations in: Research programme
Course: Research programme
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra kemije (magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Embargo expiration date: 2021-12-06
Terms of useLicence In copyright icon
Created on2019-12-18 11:58:11