The ever shorter life cycle of electronic devices and equipment is a consequence of increasingly quick development and adoption of new technologies, and a reason for exponential growth of the quantity of electrical and electronic waste, both at the global level and in the Republic of Croatia, and identical trends can be anticipated also in the future. Recycling as an integral part of the contemporary waste management system enables obtaining of secondary raw materials, whereby the quantity of waste and the space necessary for its disposal are reduced, primary raw materials are saved and environmental emissions occurring at manufacturing of new products are reduced. The basic goal striven for in recycling is to separate the different materials contained in waste into separate products which can be used as secondary raw material and which as such have a certain market value. A precondition for successful separation is to achieve liberation of different mutually (mechanically, chemically or thermally) connected materials. The success in recycling electrical and electronic waste depends on the characteristics of waste, the applied separation procedures and devices, and of course on the conditions (values of operating variables of the devices) in which separation is carried out. The first phase of the recycling process consists of manual dismantling and separation of larger parts of waste devices, whereby a larger share of iron, copper, glass and plastic materials is separated. The remaining parts need to be shredded in order to achieve liberation, and thereupon, by appropriate separation procedures, the single types of material shall be separated. In this dissertation beside enclosures and large condensers and cathode tubes containing phosphorus powder and cadmium have been manually separated from TV sets, and due to the impossibility of their save testing have been excluded from further testing. The separated wooden enclosures have been excluded from further testing, since over time contamination has occurred by harmful substances such as chrome, lead, mercury, sulphur, nickel, zinc, etc., whereas plastic enclosures contain brominated burning inhibitors, which even in very small quantities contaminate plastic materials rendering them inappropriate for obtaining new plastic. The remaining material has been divided according to its characteristics into three groups which have been tested separately. The group called „Loudspeakers“ is an integral part of the audio system and it contains the highest quantity of iron and somewhat less copper in yokes, as well as plastic, cardboard and textile. In the group „Yokes, cables, connectors and wires“ copper is represented to a high degree, and the third group of „Printed circuit boards“ contains, in addition to the copper conductor structure, also a lot of rare metals on a nonconductor basis (vitroplast, pertinax). For each of the previously indicated groups a separate test plan has been developed. For all groups shredding has been carried out first, in order to achieve liberation, followed by sieving in order to obtain classes appropriate for tests in individual separators. The test plan for air and electrostatic separation has been developed by using statistical planning of experiments under application of the programme system Statistica (Version 8, StatSoft) according to a central composite design (Central Composite Design), including 17 tests for each class on the individual device. By analysing the variance, the impact of the individual independent variable as well as the impact of the interaction of two (out of the three tested) independent variables on one (out of the two) dependent variables (concentrate quality or mass recovery), along with the assessment of this impact, has been determined. The impact of individual variables in gravitation and magnetic separation has been tested in such a way that the value of one variable was changed, while all the other variables were kept constant. Air separation tests have shown that the height of the compartment barrier has the highest impact on the quality of the concentrate, and airstream speed has the least impact, whereas with regard to the interaction of the variables, the barrier height and the position of the inlet have the highest impact. In all cases the barrier height had the highest impact on recovery. Best results (concentrate quality from 99 % to 100 % with recovery from 80 % to 99 %) were achieved at separation of grain larger than 2 mm (class 4/2 mm and 3,15/2 mm), whereas with reduced grain size separation efficiency decreased as well. By electrostatic separation high quality of concentrate has been achieved in all classes, and best results have been obtained in tests with the coarsest grain class (4/2 mm). In all tests the position of the separation knife had the largest impact on concentrate quality. Regarding interactions of the variables the interaction of the separation knife position with the voltage of the ionising electrode and the drum rotation speed had the highest impact. The results obtained by magnetic separation have shown that in most cases (in particular for coarser grain classes) wet separation is better than dry separation, whereas differences decreased with the decrease in the grain size. Best results of both the wet lowintensity and dry high-intensity separation were achieved with the smallest class, -0,5 mm. Tests of gravity concentration have shown that in order to achieve a better quality of the concentrate of better quality, concentration table should operate with smaller inclinations of the plate. Based on the obtained results a segregation scheme for electronic waste recycling has been proposed. The basic hypothesis of this dissertation, namely that the devices and procedures used in mineral processing can also be used for recycling electrical and electronic waste, has been confirmed by the results of the testing carried out.