The Republic of Croatia is proud of its rich and long viticultural history, where it plays an important social and economic role. A long tradition and the history of cultivation have influenced the assortment of vines, where autochthonous varieties play an important role. The arrival of various American diseases and phylloxera on European soil; the wine crisis and the subsequent renovation of the vineyards led to the erosion of the assortment, and the number dropped from the former 400 known autochthonous varieties to today's 100. In the last few years, interest among consumers and producers has increased and the potential of autochthonous varieties has been recognised. The 'Moslavac' and 'Belina starohrvatska' varieties are some of the Croatian autochthonous varieties where the potential for the production of grape spirits, especially brandy, has been recognised.. Wine distillates were obtained from the mentioned varieties. The production of wine distillates includes distillation on a simple or complex distillation device with a shorter column and a dephlegmator. Grape processing, microvinification and wine distillation using a complex distillation device with a column were carried out at the experiment station 'Jazbina', and wine distillation using a simple copper device was carried out in the laboratory of the Institute for Viticulture and Enology of the Faculty of Agriculture. Chemical analysis of the composition of wine was carried out using the methods prescribed by the Ordinance on physico-chemical methods of analysis of must, wine, other grape and wine products and fruit wines (N.N. 106/2004). Wine distillates shall be analysed in accordance with the Ordinance on analytical methods for spirit drinks and alcoholic beverages (N.N. 138/2005). Volatile compound concentrations are determined by the gas chromatography method. The obtained data were compared with literature data in order to assess the possibility of using these varieties for the production of brandy.